Thursday, July 30, 2009

TRICHY Chemical V SEM SYLLABUS

ANNA UNIVERSITY TIRUCHIRAPPALLI Tiruchirappalli - 620 024
Regulations 2008 Curriculum B.Tech. Chemical Engineering SEMESTER III
S.No. Subject Code Subject L T P C
Theory
1 Transforms and Partial Differential Equations 3 1 0 4
2 Electrical Drives and Control 3 0 0 3
3 Organic Chemistry 3 0 0 3
4 Mechanics of Solids 3 0 0 3
5 Fluid Mechanics 3 0 0 3
6 Environmental Science and Engineering 3 0 0 3
Practical
7 Organic Chemistry Laboratory 0 0 3 2
8 Basic Electrical Electronics Engineering Laboratory 0 0 3 2
9 Fluid Mechanics Laboratory 0 0 3 2
Total 25
ANNA UNIVERSITY TIRUCHIRAPPALLI
Tiruchirappalli - 620 024
Regulations 2008
Syllabus B.Tech. Chemical Engineering
SEMESTER III
TRANSFORMS AND PARTIAL DIFFERENTIAL EQUATIONS
LT PC 3 10 4
UNIT I FOURIERSERIES
9
Dirichlet's conditions - General Fourier series - Odd and even functions - Half range sine series -Half range cosine series - Complex form of Fourier Series - Parseval's identity - Harmonic Analysis.
UNIT II FOURIER TRANSFORMS 9
Fourier integral theorem (without proof) - Fourier transform pair - Sine and Cosine transforms - Properties - Transforms of simple functions - Convolution theorem - Parseval's identity.
UNIT III PARTIAL DIFFERENTIAL EQUATIONS 9
Formation of partial differential equations - Lagrange's linear equation - Solutions of standard types of first order partial differential equations - Linear partial differential equations of second and higher order with constant coefficients.
UNIT IV APPLICATIONS OF PARTIAL DIFFERENTIAL EQUATIONS 9
Solutions of one dimensional wave equation - One dimensional equation of heat conduction - Steady state solution of two-dimensional equation of heat conduction (Insulated edges excluded) - Fourier series solutions in cartesian coordinates.
UNIT V Z -TRANSFORMS AND DIFFERENCE EQUATIONS 9
Z transforms - Elementary properties - Inverse Z-transform - Convolution theorem - Formation of difference equations - Solution of difference equations using Z transform.
L: 45 T: 15 Total: 60
TEXT BOOK
1. Grewal B.S., "Higher Engineering Mathematics", Fortieth Edition, Khanna Publishers, 2007. REFERENCES
1. Bali.N.P and Manish Goyal, "A Textbook of Engineering Mathematic", 7th Edition, Laxmi
Publications(P) Ltd. (2007)
2 Ramana.B.V., "Higher Engineering Mathematics'", Tata Mc-GrawHill Publishing Company
limited, New Delhi (2007).
3 Glyn James, "Advanced Modern Engineering Mathematics", 3rd Edition, Pearson Education
(2007). th
4 Erwin Kreyszig, "Advanced Engineering Mathematics", 8th edition, Wiley India (2007).
ELECTRICAL DRIVES AND CONTROL
L T P C 3 0 0 3
UNIT I INTRODUCTION 8
Basic Elements - Types of Electric Drives - Factors influencing the choice of electrical drives - Heating and cooling curves - Loading conditions and classes of duty - Selection of power rating for drive motors with regard to thermal overloading and Load variation factors.
UNIT II DRIVE MOTOR CHARACTERISTICS 9
Mechanical characteristics - Speed-Torque characteristics of various types of load and drive motors -Braking of Electrical motors - DC motors: Shunt, series and compound - Single phase and three phase induction motors.
UNIT III STARTING METHODS 8
Types of D.C Motor starters - Typical control circuits for shunt and series motors - Three phase squirrel cage and slip ring induction motors.
UNIT IV CONVENTIONAL AND SOLID STATE SPEED CONTROL OF D.C. DRIVES 10
Speed control of DC series and shunt motors - Armature and field control, Ward-Leonard control system -Using controlled rectifiers and DC choppers -Applications.
UNIT V CONVENTIONAL AND SOLID STATE SPEED CONTROL OF A.C. DRIVES 10
Speed control of three phase induction motor - Voltage control, voltage / frequency control, slip power recovery scheme - Using inverters and AC voltage regulators - Applications.
TOTAL: 45
TEXT BOOKS
1. Vedam Subrahmaniam, "Electric Drives (concepts and applications)", Tata McGraw-Hill, 2001
2. Nagrath.I.J. & Kothari.D.P, "ElectricalMachines"", Tata McGraw-Hill, 1998
REFERENCES
1. Pillai.S.K "A first course on Electric drives"", Wiley Eastern Limited, 1998
2. M.D.Singh, K.B.Khanchandani, "Power Electronics"", Tata McGraw-Hill, 1998
3. H.Partab, "Art and Science and Utilisation of electrical energy"", Dhanpat Rai and Sons,
1994.
ORGANIC CHEMISTRY
LT PC 3 0 0 3
UNIT I UNIT PROCESS
Definitions - Reagents- Mechanism - Catalyst - Illustrations of the following unit process - Nitration - Halogenations - Oxidation & reduction - Esterification.
9
UNIT II ORGANIC REACTIONS MECHANISM AND ESTIMATION 9
Electrophilic reaction - Friedel craft reaction- Riemer Timenn Reaction- Nucleophilic reactions -Aldol condensation- Benzion condensation- Free radical reaction - Halogenation of Alkane-Addition HBR on Alkene in presence of peroxide.
UNIT III ORGANIC REACTIONS MECHANISM
Alylic halogination using N-Bromo succinamide (NBS) - Thermal halogenations of Alkane (CH3-CH=CH) - condensation and polymerization reaction - oxidation and reduction reactions-estimation of some organic compounds - phenol - aniline - acetone - glucose.
9
UNIT IV SYNTHETIC CHEMISTRY
Synthesis of different types of compounds like alcohol, aldehyde, acid, amine and synthesis of dicarboylic acids and unsaturated acids - Synthesis of azodyes ,methyl orange and Congo dye -Synthesis of triphenyl methane dyes - alizarin, malachite green
9
UNIT V AMINO ACIDS AND PROTEINS
Amino acids and proteins-Classification - synthesis of amino acids - Reactions of carboxyl group and amino group - Peptide linkage - End group analysis - Colour reaction of proteins- Denaturation.
9
TOTAL: 45
TEXT BOOK
1. Tiwari K.S. Vishnoi N.K. and Marhotra S.N., "A text book of Organic Chemistry", II Edition , Vikas Publishing House Pvt.Ltd., (1998), New Delhi.
REFERENCE
1. P. H. Groggins "Unit processes in organic synthesis". (Third Edition). McGraw-Hill, New York, 1947.
2. March J., "March's Advanced Organic Chemistry: Reactions, Mechanisms, and Structure", Fifth Edition, John Wiley, 2001.
3. Finar I.L., "Organic chemistry" Vol-I, Sixth Edition, Pearson Education, 2002.
MECHANICS OF SOLIDS
LT PC 3 0 0 3
UNIT I STRESS, STRAIN AND DEFORMATION OF SOLIDS 9
Rigid bodies and deformable solids - Forces on solids and supports - Equilibrium and stability -Strength and stiffness - Tension, compression and shear stresses - Hooke's law and simple problems -Compound bars - Thermal stresses - Elastic constants and Poisson's ratio - Welded joints - Design.
UNIT II TRANSVERSE LOADING ON BEAMS 9
Beams - Support conditions - Types of Beams - Transverse loading on beams - Shear force and bending moment in beams - Analysis of cantilevers, simply supported beams and over hanging beams - Relationships between loading, S.F. and B.M. In beams and their applications - S.F.& B.M. diagrams.
UNIT III DEFLECTIONS OF BEAMS 9
Double integration method - Macaulay's method - Area - moment theorems for computation of slopes and deflections in beams - conjugate beam method
UNIT IV STRESSES IN BEAMS
Theory of simple bending - Assumptions and derivation of bending equation (M/I = F/Y = E/R) -Analysis of stresses in beams - Loads carrying capacity of beams - Proportioning beam sections -Leaf springs - Flitched beams - Shear stress distribution in beams - Determination of shear stress in flanged beams.
9
UNIT V TORSION & COLUMNS 9
Torsion of circular shafts - Derivation of torsion equation (T/J = C/R = G0/L) - Stress and deformation in circular and hollow shafts - Stresses and deformation in circular and hollow shafts -Stepped shafts - Shafts fixed at both ends - Stresses in helical springs - deflection of springs - Spring constant - Axially loaded short columns - Columns of unsymmetrical sections - Euler's theory of long columns - Critical loads for prismatic columns with different end conditions - Effect of eccentricity.
TOTAL: 45
TEXT BOOKS
1. Junarkar, S.B., "Mechanics of Structure'" Vol. 1, 21st Edition, Character Publishing House, Anand, Indian, (1995)
2. William A.Nash, "Theory and Problems of Strength of Materials, Schaum's Outline Series'". McGraw Hill International Editions, Third Edition, 1994.
REFERENCE
1. Elangovan, A., Thinma Visai Iyal "Mechanics of Solids in Tamil", Anna University, Madras,
1995.
FLUID MECHANICS
LT PC 3 0 0 3
UNIT I INTRODUCTION 9
Nature of fluids - Laws of dimensional homogeneity - Physical properties of fluids - Types of fluids-Newtonian and Non Newtonian fluids- Viscosity and other secondary properties - Compressible and incompressible fluids-Hydrostatic pressure distributions- Laws of buoyancy Pressure measurements manometers
UNIT II KINEMATICS OF FLUID FLOW 9
Velocity potential- Concept of boundary layer, form drag, skin drag-Drag coefficient-Continuity, momentum and mechanical energy equations- Laminar and turbulent flow through closed conduits-Velocity profiles and friction factor for smooth and rough pipes
UNITIII DIMENSIONAL ANALYSIS AND MEASUREMENT OF FLUID FLOW 9
The principle of dimensional homogeneity - The Pi-theorem - Relationship between dimensional analysis and similitude - Use of dimensional analysis for scale up studies-Orifice meter, Venturimeter, Pitot tube, Rota meter, Weirs and notches- Principles and applications of Doppler effect in flow measurement
UNIT IV VISCOUS FLOW IN DUCTS AND BOUNDARY LAYER FLOW 9
Reynolds's number regimes-Internal versus external viscous flow- Flow in circular pipe -head loss, minor losses in pipe systems and multiple-pipe systems - Functions and pressure drag - Flow through packed and fluidized beds.
UNIT V FLOW MEASUREMENT AND TUBRO MACHINERY 9
Fluid moving machinery performance - Selection and specification- Air lift and diaphragm pump -Positive displacement pump - Reciprocating and rotary pumps - Centrifugal pump- Pump characteristics- Fans, blowers and compressors - Steam jet ejector.
TOTAL: 45
TEXT BOOKS
1. McCabe, W.L, Smith J.C and Harriot .P., "Unit Operations in Chemical Engineering", Mc-Graw-Hill, Sixth Edition, 2000.
2. Noel de Nevers, "Fluid Mechanics for Chemical Engineers'", Second Edition, McGraw-Hill, 1991.
REFERENCES rd
1. Coulson J.M. and Richardson J.E.., Chemical Engineering, Vol. 1 (3rd Edition) Pergamon Press.
2. White, F.M., "FluidMechanics", 4th Edition, McGraw-Hill Inc., 1999.
3. Daughenty, R.L., Franzini, J.B and Finnemore, E.J., "Fluid Mechanics with Engineering Applications", SI metric Edn., McGraw-Hill Book Company, 1989.
4. Darby, R. "Chemical Engineering Fluid Mechanics", Marcel Dokker, 1998.
ENVIRONMENTAL SCIENCE AND ENGINEERING
L T P C 3 0 0 3
UNIT I INTRODUCTION TO ENVIRONMENTAL STUDIES AND NATURAL
RESOURCES 9
Definition, Scope and Importance - Need For Public Awareness - Forest Resources - Use and Over -Exploitation - Deforestation - Case Studies - Timber Extraction - Mining - Dams and their Ground Water - Floods - Drought - Conflicts Over Water - Dams - Benefits and Problems - Mineral Resources - Use Effects on Forests and Tribal People - Water Resources - Use and Over-Utilization of Surface and Exploitation - Environmental Effects of Extracting and Using Mineral Resources -Case Studies - Food Resources - World Food Problems - Changes caused by Agriculture and Overgrazing - Effects of Modern Agriculture - Fertilizer - Pesticide Problems - Water Logging, salinity - Case Studies - Energy Resources - Growing Energy Needs - Renewable and Non Renewable Energy Sources - Use of Alternate Energy Sources - Case Studies - Land Resources -Land as a Resource - Land Degradation - Man Induced Landslides - Soil Erosion and Desertification - Role of an Individual in Conservation of Natural Resources - Equitable use of Resources for Sustainable Lifestyles
UNIT II ECOSYSTEMS AND BIODIVERSITY 9
Concepts of an Ecosystem - Structure and Function of an Ecosystem - Producers, Consumers and Decomposers - Energy Flow in the Ecosystem - Ecological Succession - Food Chains, Food Webs and Ecological Pyramids - Introduction, Types, Characteristic Features, Structure and Function of the (A) Forest Ecosystem (B) Grassland Ecosystem (C) Desert Ecosystem (D) Aquatic Ecosystems (Ponds, Streams, Lakes, Rivers, Oceans, Estuaries) - Introduction to Biodiversity - Definition Genetic, Species and Ecosystem Diversity - Biogeographical Classification of India - Value of Biodiversity - Consumptive Use, Productive Use, Social, Ethical, Aesthetic and Option Values -Biodiversity at Global, National and Local Levels - India as a Mega-Diversity Nation - Hot-Spots of Biodiversity - Threats to Biodiversity: Habitat Loss, Poaching of Wildlife, Man-Wildlife Conflicts -endangered and Endemic Species of India - Conservation of Biodiversity: In-Situ and Ex-Situ conservation of Biodiversity
UNIT III ENVIRONMENTAL POLLUTION 9
Definition - Causes, Effects and Control Measures of:- (A) Air Pollution (B) Water Pollution (C) Soil Pollution (D) Marine Pollution (E) Noise Pollution (F) Thermal Pollution (G) Nuclear Hazards - Solid Waste Management:- Causes, Effects and Control Measures of Urban and Industrial Wastes - Role of an Individual in Prevention of Pollution - Pollution Case Studies - disaster Management:- Floods, Earthquake, Cyclone and Landslides
UNIT IV SOCIAL ISSUES AND THE ENVIRONMENT 9
From Unsustainable To Sustainable Development - Urban Problems Related To energy - Water conservation, Rain Water Harvesting, Watershed Management - Resettlement and Rehabilitation of People, Its Problems and Concerns, Case Studies - Environmental Ethics:- Issues and Possible Solutions - Climate Change, Global Warming, Acid Rain, Ozone Layer Depletion, Nuclear Accidents and Holocaust, Case Studies - Wasteland Reclamation - Consumerism and Waste Products -Environment Production Act - Air (Prevention and Control of Pollution) Act - Water (Prevention and Control of Pollution) Act - Wildlife Protection Act - Forest Conservation Act - Issues Involved in enforcement of Environmental Legislation - Public Awareness.
UNIT V
HUMAN POPULATION AND THE ENVIRONMENT 9
Population Growth, Variation Among Nations - Population Explosion - Family Welfare Programme -Environment and Human Health - Human Rights - Value Education - HIV /AIDS - Women and Child Welfare - Role of Information Technology in Environment and Human Health - Case Studies.
Field Study of Local Area to Document Environmental assets - River/Forest/Grassland/Hill/ Mountain.
Field Study of Common Plants, Insects and Birds - Field Study of Simple Ecosystems - Pond, River, Hill Slopes, etc.
Field Study of Local Polluted Site - Urban/Rural/Industrial/Agricultural
Total: 45
TEXT BOOKS
1. Masters, G.M., "Introduction to Environmental Engineering and Science", 2nd Edition, Pearson Education, 2004.
2. Miller, T.G. Jr., "Environmental Science", Wadsworth Pub. Co.
3. Townsend C., Harper, J. and Begon, M., "Essentials of Ecology", Blackwell Science, 2003.
4. Trivedi, R.K., and Goel, P.K., "Introduction to Air Pollution", Techno-Science Publications.
REFERENCES
1. Erach, B., "The Biodiversity of India", Mapin Publishing Pvt. Ltd., Ahmedabad, India.
2. Trivedi, R.K., "Handbook of Environmental Laws, Rules, Guidelines, Compliances and Standards", Vol-I and II, Envio Media.
3. Cunningham, Cooper, W.P. and Gorhani, T.H., "Environmental Encyclopedia", Jaico Publishing House, Mumbai, 2001.
4. Wages, K.D., "Environmental Management", W.B. Saunders Co., Philadelphia, USA, 1998.
ORGANIC CHEMISTRY LABORATORY
L T P C
0 0 3 2
1. Analysis of nature of organic compounds - To identify aliphatic / aromatic, saturated / unsaturated compounds.
2. Identification and Characterization of various functional groups by their characteristic reactions: a). alcohol, b) aldehyde, c) ketone, d) carboxylic acid, e) phenol, f) ester, g) primary, secondary and tertiary amines h) amide i) nitro compounds.
3. Analysis of an unknown organic compound and preparation of suitable solid derivatives.
4. Analysis of Proteins.
5. Methodology of filtrations and recrystallization.
6. Introduction to organic Synthetic procedures:
i. Acetylation - Preparation of acetanilide from aniline.
ii. Hydrolysis - Preparation of salycilic acid from methyl salyciliate.
iii. Substitution - Conversion of acetone to iodoform.
iv. Nitration - Preparation of m-dinitrobenze from nitrobenzene.
v. Oxidation - Preparation of benzoic acid from benzaldehyde / benzylalcohol.
TOTAL: 45
REFERENCE BOOKS:
1. Vogels's "Text Book of Practical Organic Chemistry", Fifth Edition, Longman Singapore Publishers Pte. Ltd., Singapore (1989).
2. "Organic Chemistry Lab Manual, Chemistry Division", Chemical Engineering Department, A.C. Tech, Anna University (2007).
BASIC ELECTRICAL & ELECTRONICS ENGINEERING LABORATORY
LT PC 0 0 3 2
LIST OF EXPERIMENTS
1. Open circuit and load test on shunt generators
2. Load test of D.C. shunt motor
3. Load test or single phase induction motor
4. Equivalent circuit of a transformer
5. Swinturn's test
6. Load test or 3- phase squirrel cage induction motor
7. Load test or 3 -phase slip ring induction motor
8. Diode characteristics
9. Transistor amplifier
10. SCR application
11. Frequency Response Analysis
12. Characteristics of Transducers
TOTAL: 45
LIST OF EQUIPMENTS
1. Shunt Generators
2. Shunt DC motors
3. Single phase Induction motor
4. Single phase transformer
5. Three phase Squirrel Cage induction Motors
6. Diodes and Amplifiers
7. Oscilloscope
8. Transducers
FLUID MECHANICS LAB
LT PC 0 0 3 2
LIST OF EXPERIMENTS*
1. Calibration of constant and variable Head meters
2. Calibration of Weirs
3. Drag reduction studies
4. Flow through straight pipe
5. Pressure drop studies in packed column
6. Pressure drop studies in Fluidized bed
7. Flow through fittings / valves
8. Open drum orifice and draining time
9. Flow through helical coil and spiral
10. Characteristic curves of centrifugal pump
11. Characteristic curves of Gear pump
12. Characteristic curves of Reciprocating pump
13. Viscosity measurement of non Newtonian fluids
14. Flow through annulus of horizontal concentric pipe
TOTAL: 45
LIST OF EQUIPMENTS REQUIRED
1. Orifice Meter with U tube manometer
2. Venturi meter with U tube Manometer
3. V-notch and circular Notch weirs.
4. Straight pipes with U tube Manometers
5. Packed column with U tube manometer and with difference packing
6. Fluidized column with U tube manometer with different particles
7. Flow loops for pipes, fittings and valves.
8. Glass column with small spherical particles for fluidization.
9. Open drum orifice
10. Centrifugal pump with sump and pressure gauge Vertical discharge & horizontal discharge Viscometer
11. Reciprocating pump with sump and pressure gauge Vertical discharge & horizontal discharge Viscometer
12. Gear pump with sump and pressure gauge Vertical discharge & horizontal discharge Viscometer
13. Horizontal double pipe (concentric pipes) with U tube Manometer 'Minimum 10 experiments shall be offered

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