Thursday, July 30, 2009

TRICHY Petrochemical V SEM SYLLABUS

ANNA UNIVERSITY TIRUCHIRAPPALLI Tiruchirappalli - 620 024 Regulations 2007
Curriculum
B.Tech. Petrochemical Technology SEMESTER V
S.No. Subject Code Subject L T P Max. Marks
Theory
1 Special Functions 3 1 0 100
2 Heat Transfer 4 0 0 100
3 Mass Transfer Fundamentals 4 0 0 100
4 Engineering Thermodynamics 4 0 0 100
5 Natural Gas Engineering 4 0 0 100
6 Petroleum Exploration and Exploitation Techniques 3 1 0 100
Practical
7 Heat Transfer Laboratory 0 0 3 100
8 Technical Analysis Laboratory 0 0 3 100
9 Communication and Soft Skills 0 0 3 100

Laboratory




ANNA UNIVERSITY TIRUCHIRAPPALLI
Tiruchirappalli - 620 024
Regulations 2007
Syllabus
B.Tech. Petrochemical Technology
SEMESTER V
SPECIAL FUNCTIONS
LT P
3 10
UNIT I IMPROPER INTEGRALS AND SERIES SOLUTIONS 9
Improper integrals - Gamma and Beta functions - Series solutions - Ordinary point - Regular singular point of second order linear ordinary differential equation - Series solution to a second order linear ordinary differential equation about an ordinary point and a regular singular point.
UNIT II BESSEL FUNCTIONS 9
Bessel's equation - Bessel functions - Recurrence relations - Orthogonality property - Generating function - Equations reducible to Bessel's equation - Modified Bessel functions.
UNIT III LEGENDRE POLYNOMIALS 9
Legendre's equation - Legendre Polynomials - Rodrigue's formula generating function - Recurrence relations - Orthogonality property.
UNIT IV HERMITE AND LAGUERRE POLYNOMIALS 9
Hermite and Leguerre equations and their solutions - Polynomials - Rodrigue's formula -Generating functions - Recurrence relations - Orthogonality property.
UNIT V BOUNDARY VALUE PROBLEMS 9
Solution of Boundary Value Problems involving Bessel functions & Legendre polynomials.
L: 45 T: 15 Total: 60
TEXT BOOKS
1. Andrews.L.A., "Special Function for Scientist and Engineers", McGraw-Hill, 1992.
2. Narayanan, S. Manicavachagam Pillay and Ramanaiah.G, "Advanced Mathematics for Engineering Students", Vol. II S.Viswanathan Printers Private Limited, Madras, 1985.
REFERENCES
1. Grewal, B.S., "Higher Engineering Mathematics", Khanna Publishers, Delhi, 2005.
2. Jain R.K & Iyengar, S.R.K. Advanced Engineering Mathematics, Narosa Publishing House, New
Delhi, 2002.
3. N.P. Bali, N.Ch. Narayana Iyengar, "A Textbook of Engineering Mathematics", Laxmi Publications (P) Ltd., New Delhi, 6th Edn., 2004.
HEAT TRANSFER
LT P 4 0 0
UNIT I CONDUCTION 12
Modes of Heat Transfer - Steady and Unsteady state heat transfer - Concept of heat Conduction -Fourier's law of heat conduction - General Heat Conduction Equation in Spherical coordinates - One dimensional steady state heat conduction equation for flat plate, hollow cylinder, hollow sphere -Analogy between flow of heat and flow of electricity - Effect of temperature on thermal conductivity - Critical Insulation Thickness - Transient heat conduction - Lumped heat parameter model.
UNIT II CONVECTION 12
Concept of heat transfer by convection - Natural and forced convection - Concept of LMTD - Local and Overall Heat Transfer Coefficient - Application of dimensional analysis for convection -Empirical Equations for forced convection under laminar, transient and turbulent conditions -Empirical Equations for natural convection - Influence of boundary layer on heat transfer - Heat transfer through packed and fluidized beds - Heat Transfer with Phase Change: Boiling, Vaporization and Condensation.
UNIT III RADIATION 12
Concept of thermal radiations - Black body concept - Stefan Boltzman's law - Emissive power -Black body radiation - Emissivity - Planck's Law - Radiation between black surfaces - Gray surfaces - Radiation Shields - Radiation Applications - Pipe Still Heaters.
UNIT IV HEAT EXCHANGERS 12
Heat Exchanger Types - Parallel and counter flow heat exchangers - Overall heat transfer coefficient
- Log mean temperature difference for single pass - Correction factor for multi pass heat exchangers
- Heat exchanger effectiveness - Number of transfer units - Chart for different configurations - Dirt Factor.
UNIT V EVAPORATORS 12
Evaporation - Single effect and multiple effect evaporation - Boiling Point Elevation - Effect of Liquid Head - Capacity and Economy of multiple effect evaporators - Evaporation Equipments.
L: 60 Total: 60
TEXT BOOKS
1. D.S. Kumar, "Heat and Mass Transfer", S.K. Kataria & Sons, Delhi, Edition 5, 2000.
2. W. L. McCabe and J. C. Smith, "Unit Operations in Chemical Engineering", 5th Edn. McGraw Hill Publishing Co., NewDelhi, 2001.
REFERENCES
1. D. Q. Kern, "Process Heat Transfer", Tata McGraw Hill Publishing Co., New Delhi, 1990.
2. Hollman, "Heat Transfer", 8th Edn, McGraw Hill, NewDelhi, 1997.
3. F.Kreith, "Principles of Heat Transfer", 4th Edition, Harper &Row, 1976.
MASS TRANSFER FUNDAMENTALS
LT P
4 0 0
UNIT I DIFFUSION 12
Diffusion in fluids - Molecular and eddy diffusion - Measurement and calculation of diffusivities -Ordinary diffusion in multi component gaseous mixtures - Diffusion in solids - Molecular and Knudsen diffusion in solids - Theories of Mass Transfer - Film theory, penetration theory and surface renewal theories of mass transfer.
UNIT II INTERPHASE MASS TRANSFER 12
Interphase Mass Transfer - Local and overall Mass Transfer Coefficients - Steady state cocurrent and counter current mass transfer process - Stage and stage efficiencies - Concept of NTU and HTU -Equilibrium and Operating lines - JD Factor - Equipments for gas-liquid contact operations - Bubble columns - Tray towers and packed towers.
UNIT III ABSORPTION 12
Gas Absorption: principles of Absorption and Desorption - Selection of solvents for absorption -Tray tower absorber - Absorption factor - Calculation of number of theoretical stages - Murphree efficiency - Point efficiency - Tray efficiency and overall tray efficiency - Calculation of actual number of trays.
Packed tower absorber - Tower packing and characteristics - Calculation of NTU, HTU, HETP and number of stages in absorption towers - Absorption with chemical reactions.
UNIT IV DRYING 12
Drying - Principle and definitions - Estimation of drying rates, drying rate curve - Critical and equilibrium moisture content - Calculation of drying time under constant drying conditions -Different types of dryers.
UNIT-V HUMIDIFICATION AND CRYSTALLIZATION 12
Humidification - Definitions, Psychometric charts - Wet bulb temperature - Methods of humidification - Types of cooling towers, spray chambers and spray ponds.
Crystallization - Factors governing nucleation and crystal growth - Theory of Crystallization -Classification of crystallizer and their applications - Product size distribution.
L: 60 Total: 60
TEXTBOOKS
1. W.L.McCabe, J.C.Smith and P.Harriot, "Unit Operations of Chemical Engineering", 6th Edn., McGraw-Hill Book Co., New York, 2001.
2. R.E.Treybal, "Mass Transfer Operations", 3rd Edn., McGraw-Hill Book Co., New York,1980.
REFERENCES
1. J.M.Coulson and J.F.Richardson,"Chemical Engineering", Vol.I, II, III, Pergamon Press, N.Y.
1977. rd
2. C.O.Bennett, J.E.Myers, "Momentum, Heat & Mass Transfer", McGraw Hill Book Company, 3rd Edn., 1983.
3. Christie J.Geankoplis, "Transport Processes and unit operations", 3rd Edn., Prentice Hall of India
Pvt. Ltd, New Delhi, 2000.
ENGINEERING THERMODYNAMICS
LT P 4 0 0
UNIT I FUNDAMENTAL CONCEPTS AND FIRST LAW OF THERMODYNAMICS 12
Scope of thermodynamics - Basic concepts - Thermodynamic System - State and equilibrium -Process and cycles - Temperature and Zeroth law of Thermodynamics - Properties of pure substances - First law of Thermodynamics - First Law Analysis of Closed systems and control volumes and its application.
UNIT II ENTROPY AND THE SECOND LAW OF THERMODYNAMICS 12
The Clausius inequality - Entropy - Causes of entropy change - Entropy change of pure substances
- Thermal Energy reservoirs - Heat Engines - Perpetual Motion Machines - Reversible and irreversible processes - The Carnot cycle and principles - The Carnot Heat engine - The Second law Efficiency - Second law analysis of open and closed systems.
UNIT III REFRIGERATION, VAPOR & COMBINED POWER CYCLES 12
Refrigerators and Heat pumps - The Carnot refrigerator and heat pumps - The reversed Carnot cycle
- Ideal and Actual vapor compression Refrigeration cycle - Selection of right refrigerants - Heat pumps - Absorption refrigerator system - The Carnot vapor cycle - Rankine cycle - Cogeneration -Second law analysis of vapor power cycles.
UNIT IV PVT RELATIONS AND THERMODYNAMIC RELATIONS 12
PVT relations for gases and liquids - equations of state, Cubic equations of state-Thermodynamic properties from equations of state, Compressibility factor, Generalised properties of fluids-Law of corresponding state, acentric factor, gas mixtures.
Thermodynamic relations - Maxwell's relations - Estimation of thermodynamic properties-Thermodynamic properties of homogeneous mixtures - Partial molar properties, Fugacity and fugacity coefficients - Lewis and Randall rule - Property changes of mixing, activity - Excess properties, activity coefficients.
UNIT V PHASE EQUILIBRIA AND CHEMICAL REACTION EQUILIBRIA 12
Phase equilibria - Pure component and mixtures - Van Laar, Margules equation, Group contribution method - Gibb's Duhem equation - Consistency tests - Partially miscible and immiscible systems -Azeotropes - Retrograde condensation - Thermodynamic diagrams.
Chemical equilibria - Heat effects, industrial reactions - Free energy calculations - Homogeneous and heterogeneous reactions - Equilibrium composition.
L: 60 Total: 60
TEXT BOOKS
1. J.M.Smith and Van Ness, "Introduction to Engineering Thermodynamics", Ed.5, McGraw Hill,
New York, 1996.
2. K.V.Narayanan, "A Text Book of Chemical Engineering Thermodynamics", Prentice Hall of
India, New Delhi, 2002.
REFERENCES
1. Hougen and Watson , "Chemical Process Principles" Vol. II, CBS Publishers, New Delhi.2002.
2. Kyle, "Chemical and Process Thermodynamics", Ed. 2. Prentice Hall of India, New Delhi.2000.
3. Y.V.C Rao, "Chemical Engineering Thermodynamics", Universities Press, 1997.
NATURAL GAS ENGINEERING
LT P
4 0 0
UNIT I PROPERTIES AND COMPOSITION OF NATURAL GAS 12
Natural gas origin - Composition of Natural gas - Sources of Natural gas - Thermodynamics properties - Compressibility factor and chart for Natural gas - Heating value and flammability limit of Natural gas.
UNIT II ESTIMATION AND PRODUCTION OF NATURAL GAS 12
Estimation of gas reserves by Volumetric Method - Production of Natural gas - Pressure Decline Method - Problems in the Production of Natural gas - Field separation.
UNIT III GAS FROM CONDENSATE OIL FIELDS 12
Processing of Condensate well fluids - Cycling of gas condensate reservoirs - Sweep Patterns - Katy cycling plant.
UNIT IV ACID GAS TREATING OF NATURAL GAS 12
Acid gas removal: Metal oxide process - Slurry process - Amine process - Carbonate washing process - Methanol based process and other process - Sulphur recovery process.
UNIT V DEHYDRATION OF NATURAL GAS AND NGL RECOVERY
12
Dehydration: Glycol Dehydration - Solid desiccant dehydration.
NGL Recovery: Refrigeration process - Lean oil absorption process - Solid bed Adsorption and Membrane separation process - NGL fractionation.
L: 60 Total: 60
TEXT BOOKS
1. Katz and Lee "Hand Book of Natural Gas Engineering" McGraw Hill, New York 1968.
2. William C. Lyons, "Standard Handbook of Petroleum and Natural Gas Engineering", Volume 2, Gulf Professional Publishing, Elsevier Inc., 2006.
REFERENCES
1. Donald L.Katz and Robert L.Lee, Natural Gas Engineering, McGraw Hill, New York 1990
2. Dring, M. M. - The Natural Gas Industry - A review of World Resources and Industrial Applications, Butterworth, London, 1974.
3. Saied Mokhatab, William A. Poe, James G. Speight, "Handbook of Natural Gas Transmission and Processing", Gulf Professional Publishing, Elsevier Inc., 2006.
PETROLEUM EXPLORATION AND EXPLOITATION TECHNIQUES
LT P 3 10
UNIT I ORIGIN AND OCCURRENCE OF PETROLEUM AND SEDIMENTRARY
ENVIRONMENT 9
Origin of oil - Important factors that control petroleum occurrence - Migration and Accumulation -Source and Reservoir rocks - Oil bearing rocks. Continental Environment - Transitional Environment - Marine Environment.
UNIT II EXPLORATION METHODS, WELL PROGNOSIS AND ECONOMIC
ANALYSIS 9
Geological Exploration methods - Geophysical Exploration methods - Geochemical methods prognostication - Classification of Drilling Locations - Economic Analysis - Well programme -Geotechnical order.
UNIT III GEOLOGICAL STRUCTURE AND GEOLOGGING 9
Various Traps - Anticline - Fracturing - Well logging - Geological control - Gas logging - Drilling control important formation evaluation using wireline logging data.
UNIT IV DRILLING FLUIDS AND WORK COMPLETION 9
Drilling Fluids: Function, Composition, and Classicfication - Packer fluid - Casing packs - Solids removal - Completion methods - Various stimulation methods.
UNIT V OFF- SHORE TECHNOLOGY 9
Seismic Technology - Sniffer Survey - Drilling Technology - Off-share Rigs - Primary and secondary enhanced oil Recovery Techniques and methods - Major well complication and Remidies.
L: 45 T: 15 Total: 60
TEXT BOOKS
1. Bhagwan Sahay "Petroleum exploration and exploitation practices" Allied Publishers Ltd.,
Chennai, 1994.
2. Richard Dawe, "Modern petroleum Technology", Vol 1, Upstream,6th edition, John and wiley
sons Ltd, 2000.
REFERENCES
1. Howard B, Bradley, Editor, "Petroleum Engineering Handbook", Society of Petroleum Engineers, Texas, USA, 1987.
2. Nontechnical Guide to Petroleum Geology, Exploration, Drilling and Production, Norman J. Hyne, Norman J. Ph.d Hyne, 2nd edition, Pennwell Books, 2001.
3. Shay, B, et al, 1991 "Wellsite Geological Techniques for Petroleum Exploration" Allied Publishers Ltd., New Delhi.
HEAT TRANSFER LABORATORY
LT P 0 0 3
1. Determination of heat transfer coefficient using composite wall.
2. Determination of heat transfer coefficient using convection apparatus.
3. Determination of Stefan Boltzman constant using Stefan Boltzman apparatus.
4. Determination of condensing Heat transfer coefficient using vertical condenser.
5. Determination of condensing Heat transfer coefficient using horizontal condenser.
6. Study the effect of coil diameter on Heat transfer coefficient.
7. Determination of overall Heat transfer coefficient using shell and tube heat Exchanger.
8. Determination of overall Heat transfer coefficient using double pipe heat exchanger.
9. Determination of overall Heat transfer coefficient using plate type heat exchanger.
10. Study the effect of evaporation using Jacketed pan evaporator and Open pan evaporator.
Total: 45
TECHNICAL ANALYSIS LABORATORY
LT P 0 0 3
1. Oil Analysis: (3 experiments)
a) Acid value
b) Saponification value
c) Iodine value
2. Soap Analysis: (2 experiments)
a) Alkali Content
b) Fatty acid content of Soap
3. Estimation of purity of glycerol: by Dichromatic method
4. Analysis of water:
Determination chlorine demand in water: Estimation of residual chlorine in water by volumetric method
5. Cement Analysis (3 experiments)
a) Estimation of silica content
b) Estimation of calcium oxide content
c) Estimation of mixed oxide content
6. Fertilizer Analysis:
Estimation of Nitrogen in Urea by Kjeldahl method
Total: 45
COMMUNICATION AND SOFT SKILLS LABORATORY
LT P 0 0 3
Common to All Branches of III Year B.E./ B.Tech students of Anna University Tiruchirappalli and affiliated colleges)
The aim of the course is two-fold: to enable the students to develop communication skills in the language laboratory and to arrange discussions for developing soft skills in the lab and/or the classroom. Each lab session shall last for three periods.
List of activities that are to be carried out: (15 sessions x 3 periods = 45)
Lab session # 1: Listening and speaking practice exercises with communicative functions. Learning material: the ACD of Spoken English: A Foundation Course for Speakers of Indian Languages (Orient Longman, 2008)
Lab session # 2: Practice with more advanced communicative functions. Learning material: the ACD of Spoken English: A Foundation Course for Speakers of Indian Languages (Orient Longman, 2008)
Lab session # 3: Pronunciation exercises with Oxford Advanced Learners' Dictionary of Current English or any other standard Dictionary
Lab session # 4: Making an oral presentation in English. Learning Material: Professional Presentations VCD (Cambridge University Press)
Lab session # 5: Listening to telephone conversations in English and completing the tasks. Learning material: Essential Telephoning in English ACD (Cambridge University Press)
Lab session # 6: Giving an exposure to and practice with model group discussion and interviews. Learning material: How to Prepare for Group Discussion and Interview Audio Cassette (McGraw-
Hill)
Lab session # 7: Giving insights into the format and the task types in the IELTS (International English Language Testing System). Learning Material: Objective IELTS, Intermediate Level (CUP)
Lab session # 8: Understanding the format and the task types in the TOEFL (Test of English as a Foreign Language). Learning Material: Understanding the TOEFL (Educational Testing Services, Princeton)
Lab session # 9: Administering the BEC (Business English Certificate) Diagnostic Test. Learning Material: BEC Practice Materials (British Council, Chennai)
Lab session # 10: Completing the steps involved in Career, Life Planning and Change Management. Learning Material: Developing Soft Skills (Pearson Education)
Lab session # 11: Setting goals and objectives exercises. Learning Material: Developing Soft Skills (Pearson Education)
Lab session # 12: Prioritizing and time planning exercises. Learning Material: Managing Time Multimedia Program CD
Lab session # 13: Taking a Personality Typing/ Psychometric Test Learning Material: 200 Psychometric Test prepared by the CUIC, Anna University Chennai
Lab session # 14: Critical and creative thinking exercises.
Lab session # 15: Improving body language and cross-cultural communication with pictures. Learning material: Body Language (S. Chand and Co.) For a detailed plan, refer to the topics given below;
UNIT I LISTENING AND SPEAKING PRACTICE IN COMMUNICATIVE
FUNCTIONS
Introductions and meetings - Talking about studies and/ or job - Expressing likes and dislikes -Describing daily routines and current activities - Talking about past states and events - Talking about future plans and intentions - Expressing preferences - Giving reasons - Expressing opinions, agreement and disagreement - Seeking and giving advice - Making suggestions
UNIT II SPEAKING APPLICATIONS
Making an oral presentation - Preparing the presentation - Performing the presentation - Beginning - Language - Visual aids and body language - Voice - Ending - Questions - Telephone conversations - Group Discussion and Interview
UNIT III UNDERSTANDING AND PREPARING FOR INTERNATIONAL ENGLISH LANGUAGE EXAMINATIONS
Graded Examinations in Spoken English (GESE) - Spoken English for Work (SEW) - International English Language Testing System (IELTS) - Test of English as a Foreign Language (TOEFL) -Business English Certificate (BEC)
UNIT IV SOFT SKILLS (1)
Preparing for and dealing with change - Motivation, goal-setting and self-esteem - Managing time and stress - Career and life planning - Team work - Leadership traits
UNIT V SOFT SKILLS (2)
Multiple Intelligences - Learning Styles and Personality typing - Critical and creative thinking -People, cultures and self - Intercultural Communication
RESOURCES
1. Kamalesh Sadanand and Susheela Punitha, "Spoken English: A Foundation Course" for Speakers of Indian Languages, Part 2 Audio CD, Hyderabad: Orient Longman, 2008
2. Malcome Goodale, "Professional Presentations", (VCD) New Delhi: Cambridge University
Press, 2005
3. Barbara Garside and Tony Garside, Essential Telephoning in English (Audio CD), Cambridge: Cambridge University Press, 2002
4. Hari Mohan Prasad and Rajnish Mohan, How to Prepare for Group Discussion and Interview (Audio Cassette) Tata McGraw-Hill Publishing
5. Graded Examinations in Spoken English and Spoken English for Work downloadable materials from Trinity College, London
6. International English Language Testing System Practice Tests, CUP
7. Business English Certificate Materials, Cambridge University Press
8. Personality Development (CD-ROM), Times Multimedia, Mumbai
9. Interactive Multimedia Programs on Managing Time and Stress
10. Robert M. Sherfield and et al "Developing Soft Skills" 4th edition, New Delhi: Pearson
Education, 2009
Total: 45

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