TRICHY Petrochemical 3rd SEM SYLLABUS

ANNA UNIVERSITY TIRUCHIRAPPALLI Tiruchirappalli - 620 024
Regulations 2008
CURRICULUM
B.TECH. PETROCHEMICAL TECHNOLOGY
SEMESTER III
S.No. Subject Code Subject L T P C
Theory
1 Transforms and Partial Differential Equations 3 1 0 4
2 Organic Chemistry 3 0 0 3
3 Environmental Science and Engineering 3 0 0 3
4 Industrial Chemical Technology 3 0 0 3
5 Electrical Drives and Control 3 0 0 3
6 Data Structures 3 0 0 3
Practical
7 Organic Chemistry Laboratory 0 0 3 2
8 Electrical Machines Laboratory 0 0 3 2
9 Data Structures Laboratory 0 0 3 2
Total 25
ANNA UNIVERSITY TIRUCHIRAPPALLI Tiruchirappalli - 620 024
Regulations 2008 Syllabus
B.TECH. PETROCHEMICAL TECHNOLOGY SEMESTER III
TRANSFORMS AND PARTIAL DIFFERENTIAL EQUATIONS
L T P C 3 10 4
UNIT I FOURIER SERIES 9
Dirichlet's conditions - General Fourier series - Odd and even functions - Half range sine series -Half range cosine series - Complex form of Fourier Series - Parseval's identity - Harmonic
Analysis.
UNIT II FOURIER TRANSFORM 9
Fourier integral theorem (without proof) - Fourier transform pair - Sine and
Cosine transforms - Properties - Transforms of simple functions - Convolution theorem -Parseval's identity.
UNIT III PARTIAL DIFFERENTIAL EQUATIONS 9
Formation of partial differential equations - Lagrange's linear equation - Solution of standard types of first order partial differential equations - Linear partial differential equations of second and higher order with constant coefficients
UNIT IV APPLICATIONS OF PARTIAL DIFFERENTIAL EQUATIONS 9
Solutions of one dimensional wave equation - One dimensional equation of heat conduction -Steady state solution of two-dimensional equation of heat equation (Insulated edges excluded) -Fourier series solutions in cartesian coordinates.
UNIT V Z-TRANSFORM AND DIFFERENCE EQUATIONS 9
Z-transform - Elementary properties - Inverse Z-transform - Convolution theorem - Formation of difference equations - Solution of difference equations using Z-transform
L: 45 T: 15 Total: 60
TEXTBOOK
1. Grewal B.S, "Higher Engineering Mathematics", 39th Edition, Khanna Publishers, Delhi, 2007.
REFERENCES th
1. Bali.N.P., Manish Goyal, "A Textbook of Engineering Mathematics", 7th Edition, Laxmi Publications (P) Ltd.
2. Ramana.B.V. "Higher Engineering Mathematics" Tata McGraw Hill, New Delhi
3. Glyn James, "Advanced Modern Engineering Mathematics", 3rd Edition, Pearson Education,
2007.
4. Erwin Kreyszig, "Advanced Engineering Mathematics" 8th Edition, Wiley India, 2007.
ORGANIC CHEMISTRY
L T P C
3 0 0 3
UNIT I ALIPHATIC HYDROCARBONS AND ALCOHOLS 9
Alkanes - General methods of preparation - Physical and chemical properties - Alkenes - General methods of preparation - Physical and chemical properties - Markovnikov's rule - Peroxide effect -Bayer's test - Alkynes - General methods of preparation and properties monohydric alcohols -Saytzeff rule - Methods of distinguishing the three classes of alcohols - Lucas test - Dichromate test.
UNIT II ALDEHYDES, KETONES AND ACIDS 9
General methods of preparation - Physical and chemical properties - Aldol condensation -Clemmensen reduction - Wolf-Kishner reduction - Haloform reaction - Cannizzaro reaction -Reformatsky reaction - Wittig reaction - Saturated monocarbozylic acids - Methods of preparation - Physical and chemical properties - Hell-Volhard-Zelinsky reaction - Amino acids - Methods of preparation - Physical and chemical properties.
UNIT III CARBOHYDRATES 9
Classification of carbohydrates - Monosaccharides - Reactions of glucose and fructose - Open chain and cyclic structures of glucose and fructose - Mutarotation - Epimerization - Killiani-Fisher synthesis - Ruff degradation - Conversion of aldoses to ketoses and ketoses to aldoses -Disaccharides - Properties and structure of sucrose - Polysaccharides - Properties and structure of starch and cellulose - Derivatives of cellulose - Carboxy methyl cellulose and gun cotton.
UNIT IV AROMATIC HYDROCARBON, AMINE AND DIAZONIUM SALT 9
Benzene - Aromaticity - Huckel rule - General methods of preparation of benzene - Electrophilic substitution reactions - Directive effects of substituents - Aromatic amino compounds - General methods of preparation - Physical and chemical properties - Carbylamines reaction -Aryldiazonium salts - Preparation and synthetic applications.
UNIT V DYES AND DYEING 9
Colour and constitution - Synthesis - Azodyes - Methyl orange - Methyl red and Congo red -Triphenylmethane dyes - Malachite green - Para-rosaniline - Alizarin - Eosin - Introduction to natural and reactive dyes.
Total: 45
TEXT BOOKS
1. Morrison R.T. and Boyd R.N., "Organic chemistry'", Sixth Edition, Prentice Hall of India (P)
Ltd., 2003.
2. Arun Bahl and Bahl B.S., "Advanced Organic Chemistry", Sixteenth Edition, S.Chand &
Company Ltd., 2002.
REFERENCES
1. March J., "MarchS Advanced Organic Chemistry: Reactions, Mechanisms, and Structure'",
Fifth Edition, John Wiley, 2001.
2. Finar I.L., "Organic chemistry" Vol-I, Sixth Edition, Pearson Education, 2002.
3. Sharma B.K., "Industrial Chemistry", Twelfth Edition, Goel Publishing house, 2001.
ENVIRONMENTAL SCIENCE AND ENGINEERING
L T P C 3 0 0 3
UNIT I INTRODUCTION TO ENVIRONMENTAL STUDIES AND NATURAL RESOURCES 9
Definition, Scope and Importance - Need For Public Awareness - Forest Resources - Use and Over
- Exploitation - Deforestation - Case Studies - Timber Extraction - Mining - Dams and their Ground Water - Floods - Drought - Conflicts Over Water - Dams - Benefits and Problems -Mineral Resources - Use Effects on Forests and Tribal People - Water Resources - Use and Over-Utilization of Surface and Exploitation - Environmental Effects of Extracting and Using Mineral Resources - Case Studies - Food Resources - World Food Problems - Changes caused by Agriculture and Overgrazing - Effects of Modern Agriculture - Fertilizer - Pesticide Problems -Water Logging, salinity - Case Studies - Energy Resources - Growing Energy Needs - Renewable and Non Renewable Energy Sources - Use of Alternate Energy Sources - Case Studies - Land Resources - Land as a Resource - Land Degradation - Man Induced Landslides - Soil Erosion and Desertification - Role of an Individual in Conservation of Natural Resources - Equitable use of Resources for Sustainable Lifestyles
UNIT II ECOSYSTEMS AND BIODIVERSITY 9
Concepts of an Ecosystem - Structure and Function of an Ecosystem - Producers, Consumers and Decomposers - Energy Flow in the Ecosystem - Ecological Succession - Food Chains, Food Webs and Ecological Pyramids - Introduction, Types, Characteristic Features, Structure and Function of the (A) Forest Ecosystem (B) Grassland Ecosystem (C) Desert Ecosystem (D) Aquatic Ecosystems (Ponds, Streams, Lakes, Rivers, Oceans, Estuaries) - Introduction to Biodiversity - Definition Genetic, Species and Ecosystem Diversity - Biogeographical Classification of India - Value of Biodiversity - Consumptive Use, Productive Use, Social, Ethical, Aesthetic and Option Values -Biodiversity at Global, National and Local Levels - India as a Mega-Diversity Nation - Hot-Spots of Biodiversity - Threats to Biodiversity: Habitat Loss, Poaching of Wildlife, Man-Wildlife Conflicts -endangered and Endemic Species of India - Conservation of Biodiversity: In-Situ and Ex-Situ conservation of Biodiversity
UNIT III ENVIRONMENTAL POLLUTION 9
Definition - Causes, Effects and Control Measures of:- (A) Air Pollution (B) Water Pollution (C) Soil Pollution (D) Marine Pollution (E) Noise Pollution (F) Thermal Pollution (G) Nuclear Hazards
- Solid Waste Management:- Causes, Effects and Control Measures of Urban and Industrial Wastes
- Role of an Individual in Prevention of Pollution - Pollution Case Studies - disaster Management:-Floods, Earthquake, Cyclone and Landslides
UNIT IV SOCIAL ISSUES AND THE ENVIRONMENT 9
From Unsustainable To Sustainable Development - Urban Problems Related To energy - Water conservation, Rain Water Harvesting, Watershed Management - Resettlement and Rehabilitation of People, Its Problems and Concerns, Case Studies - Environmental Ethics:- Issues and Possible Solutions - Climate Change, Global Warming, Acid Rain, Ozone Layer Depletion, Nuclear Accidents and Holocaust, Case Studies - Wasteland Reclamation - Consumerism and Waste Products - Environment Production Act - Air (Prevention and Control of Pollution) Act - Water (Prevention and Control of Pollution) Act - Wildlife Protection Act - Forest Conservation Act -Issues Involved in enforcement of Environmental Legislation - Public Awareness.
UNIT V HUMAN POPULATION AND THE ENVIRONMENT 9
Population Growth, Variation Among Nations - Population Explosion - Family Welfare Programme - Environment and Human Health - Human Rights - Value Education - HIV /AIDS - Women and Child Welfare - Role of Information Technology in Environment and Human Health - Case Studies.
Field Study of Local Area to Document Environmental assets - River/Forest/Grassland/Hill/ Mountain.
Field Study of Common Plants, Insects and Birds - Field Study of Simple Ecosystems - Pond, River, Hill Slopes, etc.
Field Study of Local Polluted Site - Urban/Rural/Industrial/Agricultural
Total: 45
TEXT BOOKS
1. Masters, G.M., "Introduction to Environmental Engineering and Science", 2nd Edition, Pearson Education, 2004.
2. Miller, T.G. Jr., "Environmental Science", Wadsworth Pub. Co.
3. Townsend C., Harper, J. and Begon, M., "Essentials of Ecology", Blackwell Science,
2003.
4. Trivedi, R.K., and Goel, P.K., "Introduction to Air Pollution", Techno-Science Publications.
REFERENCES
1. Erach, B., "The Biodiversity of India", Mapin Publishing Pvt. Ltd., Ahmedabad, India.
2. Trivedi, R.K., "Handbook of Environmental Laws, Rules, Guidelines, Compliances and Standards", Vol-I and II, Envio Media.
3. Cunningham, Cooper, W.P. and Gorhani, T.H., "Environmental Encyclopedia", Jaico Publishing House, Mumbai, 2001.
4. Wages, K.D., "Environmental Management", W.B. Saunders Co., Philadelphia, USA, 1998.
INDUSTRIAL CHEMICAL TECHNOLOGY
LT P C
3 0 0 3
UNIT I ALKALIES 9
Chloro-alkali industries - Manufacture of Soda ash - Caustic Soda - Chlorine.
UNIT II ACIDS 9
Manufacture of Sulphuric acid - Hydrochloric acid - Phosphoric acid - Nitric acid.
UNIT III GLASSES 9
Manufacture of glasses - Special glasses - Ceramics and Refractories - Paints and Pigments.
UNIT IV INDUSTRIAL GASES 9
Carbon dioxide - Nitrogen - Hydrogen - Oxygen and Acetylene.
UNIT V FERTILIZERS 9
Nitrogen fertilizers - Synthetic ammonia - Urea - Ammonium chloride - CAN - Ammonium sulphate - Phosphorous fertilizers - Phosphate rock - Super phosphate - Triple Super Phosphate -MAP and DAP - Potassium fertilizers - Potassium chloride - Potassium sulphate.
Total: 45
TEXT BOOKS
1. Austin G.T., "Shreve's Chemical Process Industries", Fifth Edition, McGraw Hill, 1998.
2. Gopala Rao M. and Sittig M., "Dryden's Outlines of Chemical Technology for the 21st Century", Third Edition, Affiliated East-West press, 2007.
REFERENCES
1. Shukla S.D. and Pandey G.N., "Text book of Chemical Technology" Vol-I, Vikas publishing house (P) Ltd., 1977.
2. Sharma B.K., "Industrial Chemistry", Twelfth Edition, Goel Publishing house, 2001.
3. Pandey G.N., "Text Book of Chemical Technology" Vikas publishing house (P) Ltd., 1992.
ELECTRICAL DRIVES AND CONTROL
(Common to Mechanical, Production and Petrochemical technology)
LT P C 3 0 0 3
UNIT I INTRODUCTION 9
Basic Elements - Types of Electric Drives - factors influencing the choice of electrical drives - heating and cooling curves - Loading conditions and classes of duty - Selection of power rating for drive motors with regard to thermal overloading and Load variation factors
UNIT II MOTOR CHARACTERISTICS 9
Mechanical characteristics - Speed-Torque characteristics of various types of load and drive motors -Braking of Electrical motors - DC motors: Shunt, series and compound - single phase and three phase induction motors.
UNIT III STARTING METHODS 9
Types of D.C Motor starters - Typical control circuits for shunt and series motors - Three phase squirrel cage and slip ring induction motors.
UNIT IV CONVENTIONAL AND SOLID STATE SPEED CONTROL OF D.C. DRIVES
9
Speed control of DC series and shunt motors - Armature and field control, Ward-Leonard control system -Using controlled rectifiers and DC choppers -applications.
UNIT V CONVENTIONAL AND SOLID STATE SPEED CONTROL OF A.C. DRIVES
9
Speed control of three phase induction motor - Voltage control, voltage / frequency control, slip power recovery scheme - Using inverters and AC voltage regulators - applications.
Total: 45
TEXT BOOKS
1. Vedam Subrahmaniam, "Electric Drives (concepts and applications)", Tata McGraw-Hill, 2001.
2. Nagrath.IJ. & Kothari.D.P, "ElectricalMachines", Tata McGraw-Hill, 1998.
REFERENCES
1. Pillai.S.K "A first course on Electric drives", Wiley Eastern Limited, 1998
2. M.D.Singh, K.B.Khanchandani, "Power Electronics", Tata McGraw-Hill, 1998
3. H.Partab, "Art and Science and Utilisation of electrical energy", Dhanpat Rai and Sons, 1994.
DATA STRUCTURES
L T P C 3 0 0 3
UNIT I FUNDAMENTALS OF ALGORITHMS 8
Algorithm - Analysis of Algorithm - Best Case and Worst Case Complexities - Analysis of Algorithm using Data Structures - Performance Analysis - Time Complexity - Space Complexity -Amortized Time Complexity - Asymptotic Notation
UNIT II FUNDAMENTALS OF DATA STRUCTURES 9
Arrays - Structures - Stacks - Definition and examples - Representing Stacks - Queues and Lists -Queue and its Representation - Applications of Stack - Queue and Linked Lists.
UNIT III TREES 10
Binary Trees - Operations on Binary Tree Representations - Node Representation - Internal and External Nodes - Implicit Array Representation - Binary Tree Traversal - Huffman Algorithm -Representing Lists as Binary Trees - Sorting and Searching Techniques - Tree Searching - Hashing
UNIT IV GRAPHS AND THEIR APPLICATIONS 9
Graphs - An Application of Graphs - Representation - Transitive Closure - Warshall's Algorithm -Shortest path Algorithm - A Flow Problem - Dijikstra's Algorithm - Minimum Spanning Trees -Kruskal and Prim's Algorithm - An Application of Scheduling - Linked Representation of Graphs -Graph Traversals
UNIT V STORAGE MANAGEMENT 9
General Lists - Operations - Linked List Representation - Using Lists - Freeing List Nodes -Automatic List Management : Reference Count Method - Garbage Collection - Collection and Compaction
Total: 45
TEXT BOOKS
1. Cormen T. H.., Leiserson C. E, and Rivest R.L., "Introduction to Algorithms", Prentice Hall of India, New Delhi, 2007.
2. M.A.Weiss, "Data Structures and Algorithm Analysis in C", Second Edition, Pearson Education, 2005.
REFERENCES
1. Ellis Horowitz, Sartaj Sahni and Sanguthevar Rajasekaran, "Computer Algorthims/C++", Universities Press (India) Private Limited, Second Edition, 2007.
2. A. V. Aho, J. E. Hopcroft, and J. D. Ullman, "Data Structures and Algorithms", First Edition, Pearson Education, 2003.
3. R. F. Gilberg and B. A. Forouzan, "Data Structures", Second Edition, Thomson India
Edition, 2005.
4. Robert L Kruse, Bruce P Leung and Clovin L Tondo, "Data Structures and Program Design
in C", Pearson Education, 2004.
5. Tanaenbaum A. S. Langram, Y. Augestein M.J, "Data Structures using C", Pearson
Education, 2004.
ORGANIC CHEMISTRY LABORATORY
L T P C
0 0 3 2
1. Estimation of Alcohol
2. Estimation of Aldehydes & Ketones
3. Estimation of Phenol
4. Pigment Analysis
5. Ore/Alloys analysis
6. Estimation of Amines
7. Estimation of Glucose
8. Preparation of Asprin
9. Preparation of Methyl orange
10. Preparation of Schiff's base
11. Synthesis of Porphyrin
12. Qualitative analysis of simple Organic compounds.
13. Polymer Analysis
14. Hydrolysis of Sucrose.
15. Industrial Waste Water analysis
Total: 45
ELECTRICAL MACHINES LABORATORY
L T P C 0 0 3 2
1. Open circuit and load characteristics of separately excited and self excited D.C. generator
2. Load test on D.C. shunt motor
3. Load test on D.C. series motor
4. Speed control of D.C. shunt motor
5. Load test on single phase transformer and open circuit and short circuit test on single phase transformer
6. Regulation of three phase alternator by E.M.F. and M.M.F. methods
7. Load test on three phase induction motor
8. No load and blocked rotor tests on three phase induction motor (Determination of equivalent circuit parameters)
9. Load test on single- phase induction motor
10. Study of D.C. motor and induction motor starters
Total: 45
DATA STRUCTURES LABORATORY
L T P C 0 0 3 2
LIST OF EXPERIMENTS
1) Implement singly and doubly linked lists.
2) Represent a polynomial as a linked list and write functions for polynomial addition.
3) Implement stack and use it to convert infix to postfix expression
4) Implement a double-ended queue (dequeue) where insertion and deletion operations are possible at both the ends.
5) Implement an expression tree. Produce its pre-order, in-order, and post-order traversals.
6) Implement binary search tree.
7) Implement insertion in AVL trees.
8) Implement priority queue using binary heaps
9) Implement hashing with open addressing.
10) Implement Prim's algorithm using priority queues to find MST of an undirected graph.
Total: 45